C₅₅H₇₁NO₁₂

Base Information

Chemical Name:C₅₅H₇₁NO₁₂
CAS No.:1448230-75-8
Molecular Formula:C₅₅H₇₁NO₁₂
Molecular Weight:938.168
Hs Code.:

C<sub>55</sub>H<sub>71</sub>NO<sub>12</sub>

Synonyms:C₅₅H₇₁NO₁₂

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Chemical Property of C₅₅H₇₁NO₁₂

Chemical Property:

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Technology Process of C₅₅H₇₁NO₁₂

There total 14 articles about C₅₅H₇₁NO₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₅₆O₉

: 101711-78-8,131685-53-5
(3R)-3-propionyl-4-benzyloxazolidin-2-one

: 1448230-75-8
C₅₅H₇₁NO₁₂

Guidance literature:: (3R)-3-propionyl-4-benzyloxazolidin-2-one; With di-n-butylboryl trifluoromethanesulfonate; triethylamine; In dichloromethane; at 0 ℃; for 1h;

C₄₂H₅₆O₉; In dichloromethane; at -78 - 0 ℃; for 2.25h;

With dihydrogen peroxide; In methanol; dichloromethane; water; at 0 ℃; for 1h;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-65-6
C₃₂H₆₇IO₄Si₂

: 1448230-75-8
C₅₅H₇₁NO₁₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

1.2: 0.33 h / 20 °C

1.3: 13 h / 50 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

3.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

4.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

5.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

6.2: 12 h / 0 - 20 °C

7.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

8.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C

9.1: triethylamine; di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C

9.2: 2.25 h / -78 - 0 °C

9.3: 1 h / 0 °C

With di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; acetic acid; triethylamine; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; pentane; 9.1: |Evans Aldol Reaction / 9.2: |Evans Aldol Reaction;
DOI:10.1021/ol4017518

Reference yield:

: 1448230-61-2
C₂₂H₃₆O₆

: 1448230-75-8
C₅₅H₇₁NO₁₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1.17 h / 20 °C / pH 7

3.1: triethylamine; dmap / dichloromethane / 25 h / 0 - 20 °C

4.1: sodium iodide / acetone / 18 h / 50 °C

5.1: 9-methoxy-9-BBN; tert.-butyl lithium / tetrahydrofuran; hexane; diethyl ether; pentane / 4 h / -78 - 20 °C

5.2: 0.33 h / 20 °C

5.3: 13 h / 50 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C

7.1: pyridinium p-toluenesulfonate / dichloromethane / 7.5 h / 0 - 20 °C

8.1: acetic acid / tetrahydrofuran; water / 16 h / 20 °C

9.1: pyridinium p-toluenesulfonate / dichloromethane / 2 h / 20 °C

10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 - 20 °C

10.2: 12 h / 0 - 20 °C

11.1: diisobutylaluminium hydride / dichloromethane; hexane / 2.25 h / -78 °C

12.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 °C

13.1: triethylamine; di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 1 h / 0 °C

13.2: 2.25 h / -78 - 0 °C

13.3: 1 h / 0 °C

With 2,6-dimethylpyridine; dmap; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; tert.-butyl lithium; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; acetic acid; triethylamine; 9-methoxy-9-BBN; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium iodide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; mineral oil; pentane; 13.1: |Evans Aldol Reaction / 13.2: |Evans Aldol Reaction;
DOI:10.1021/ol4017518