4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester

Base Information

Chemical Name:4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester
CAS No.:864970-94-5
Molecular Formula:C₂₂H₂₉F₄N₃O₃S
Molecular Weight:491.55
Hs Code.:

Synonyms:4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester

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Chemical Property of 4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester

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Technology Process of 4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester

There total 2 articles about 4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.9%

: 864970-89-8
12-hydroxy-dodecanethioic acid S-propyl ester

: 122590-77-6
4-azido-2,3,5,6-tetrafluorobenzoic acid

: 864970-94-5
4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tetlet.2005.06.125

Reference yield:

: 505-95-3
12-hydroxydodecanoic acid

: 864970-94-5
4-azido-2,3,5,6-tetrafluoro-benzoic acid 11-propylsulfanylcarbonyl-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DCC / acetonitrile

2: 80.9 percent / DCC; DMAP / CH₂Cl₂

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; acetonitrile;
DOI:10.1016/j.tetlet.2005.06.125