2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Chemical Name:2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone
CAS No.:514801-73-1
Molecular Formula:C₅₀H₄₂N₆O₈
Molecular Weight:854.919
Hs Code.:

2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1<i>H</i>,3<i>H</i>-benzo[<i>de</i>]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[<i>lmn</i>][3,8]phenanthroline-1,3,6,8-tetraone

Synonyms:2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Chemical Property of 2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

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Technology Process of 2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

There total 3 articles about 2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 203915-43-9
7-octyl-1H-isochromeno[6,5,4-def]isoquinoline-1,3,6,8(7H)-tetraone

: 2-(3-amino-phenyl)-6-[4-(4-nitro-phenyl)-piperazin-1-yl]-benzo[de]isoquinoline-1,3-dione

: 514801-73-1
2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: With 1H-imidazole; In chloroform; for 4h; Heating;
DOI:10.1021/ja029062a

Reference yield:

: 6269-89-2
1-(4-Nitrophenyl)piperazine

: 514801-73-1
2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / N,N-dimethyl-acetamide / 3 h / 130 °C

2: 85 percent / imidazole / CHCl₃ / 4 h / Heating

With 1H-imidazole; In chloroform; N,N-dimethyl acetamide;
DOI:10.1021/ja029062a

Reference yield:

: 259656-00-3
N-(3-aminophenyl)-4-bromonaphthalene-1,8-dicarboximide

: 514801-73-1
2-(3-{6-[4-(4-nitro-phenyl)-piperazin-1-yl]-1,3-dioxo-1H,3H-benzo[de]isoquinolin-2-yl}-phenyl)-7-octyl-benzo[lmn][3,8]phenanthroline-1,3,6,8-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / N,N-dimethyl-acetamide / 3 h / 130 °C

2: 85 percent / imidazole / CHCl₃ / 4 h / Heating

With 1H-imidazole; In chloroform; N,N-dimethyl acetamide;
DOI:10.1021/ja029062a