(Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester

Base Information

Chemical Name:(Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester
CAS No.:73972-28-8
Molecular Formula:C₁₃H₁₅NO₃S
Molecular Weight:265.333
Hs Code.:

Synonyms:(Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester

Suppliers and Price of (Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester

There total 2 articles about (Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 60084-47-1
(Z)-β-Chloro-N-acetyldehydroalanine methyl ester

: 100-53-8
phenylmethanethiol

: 73972-28-8
(Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester

Guidance literature:: With triethylamine; In acetonitrile; Ambient temperature;
DOI:10.1021/jo01304a020

Reference yield:

: 35356-70-8
Methyl 2-acetamidoacrylate

: 73972-28-8
(Z)-N-Acetyl-β-(benzylthio)-α,β-didehydroalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) chlorine 2) DBU / 1) CCl₄ 2) methylene chloride, 20 min room temperature

2: 64 percent / triethylamine / acetonitrile / Ambient temperature

With chlorine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In acetonitrile;
DOI:10.1021/jo01304a020