N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

Base Information

• Chemical Name: N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal
• CAS No.: 79539-44-9
• Molecular Formula: C₄₅H₅₁NO₉
• Molecular Weight: 749.901

Synonyms:N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

Chemical Property of N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

There total 3 articles about N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

benzyl chloroformate (501-53-1,94274-21-2) + N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (76992-52-4) → N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (79539-44-9)

Guidance literature:

With sodium hydrogencarbonate; In chloroform; water; 2 deg C, 0.5 h, room temp. 1 h;

DOI:10.1248/cpb.30.3197

Reference yield:

[1-(3,5-Bis-benzyloxy-phenyl)-meth-(Z)-ylidene]-(2,2-diethoxy-ethyl)-amine (60095-69-4) → N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (79539-44-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Mg / tetrahydrofuran / 1 h / Heating

2: 84 percent / NaHCO₃ / CHCl₃; H₂O / 2 deg C, 0.5 h, room temp. 1 h

With sodium hydrogencarbonate; magnesium; In tetrahydrofuran; chloroform; water;

DOI:10.1248/cpb.30.3197

Reference yield:

5-(chloromethyl)-1,2,3-trimethoxybenzene (3840-30-0) → N-benzyloxycarbonyl-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal (79539-44-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Mg / tetrahydrofuran / 1 h / Heating

2: 84 percent / NaHCO₃ / CHCl₃; H₂O / 2 deg C, 0.5 h, room temp. 1 h

With sodium hydrogencarbonate; magnesium; In tetrahydrofuran; chloroform; water;

DOI:10.1248/cpb.30.3197

upstream raw materials:

benzyl chloroformate

N-<α-(3,5-dibenzyloxyphenyl)-β-(3,4,5-trimethoxyphenyl)>ethylaminoacetaldehyde diethyl acetal

[1-(3,5-Bis-benzyloxy-phenyl)-meth-(Z)-ylidene]-(2,2-diethoxy-ethyl)-amine

5-(chloromethyl)-1,2,3-trimethoxybenzene

Downstream raw materials:

C₄₁H₃₉NO₇

(+/-)-TA-073

C₄₁H₃₉NO₇

N-benzyloxycarbonyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2-dihydroisoquinoline

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