N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

Base Information

Chemical Name:N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine
CAS No.:88287-97-2
Molecular Formula:C₄₃H₄₉N₃O₁₁
Molecular Weight:783.876
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

Suppliers and Price of N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

There total 8 articles about N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 88287-96-1
N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine allyl ester

: 88287-97-2
N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 0.5h; Ambient temperature;
DOI:10.1021/jo00265a007

Reference yield:

: 88287-95-0
(S)-2-((S)-2-Amino-propionylamino)-propionic acid allyl ester; hydrochloride

: 88287-97-2
N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NEt₃, EEDQ / CH₂Cl₂

2: 97 percent / morpholin / (Ph₃P)4Pd / tetrahydrofuran

With morpholine; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;

Reference yield:

: 88295-41-4
N-(benzyloxycarbonyl)serine allyl ester

: 88287-97-2
N-(benzyloxycarbonyl)-O-(2,3,4-tri-O-benzyl-β-D-xylopyranosyl)serylalanylalanine

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / BF₃ / -30 °C

2: 97 percent / morpholin / 10percent (Ph₃P)4Pd / tetrahydrofuran / 0.5 h / Ambient temperature

3: 87 percent / NEt₃, EEDQ / CH₂Cl₂

4: 97 percent / morpholin / (Ph₃P)4Pd / tetrahydrofuran

With morpholine; boron trifluoride; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; dichloromethane;