Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate

Base Information

• Chemical Name: Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate
• CAS No.: 85539-39-5
• Molecular Formula: C₁₆H₂₂NO₆S₂*Na
• Molecular Weight: 411.476

Synonyms:Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate

Chemical Property of Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate

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Technology Process of Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate

There total 2 articles about Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

(1S,5R,7S)-3-(Toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]nonane-7-carbaldehyde (33343-77-0) → Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate (85539-39-5)

Guidance literature:

With sodium hydrogen sulfate; In ethanol; water;

DOI:10.1016/S0040-4039(00)85649-X

Reference yield:

[(1S,5R,7S)-3-(Toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanol (33366-53-9) → Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate (85539-39-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Pyridinium chlorochromate, NaOAc

2: 63 percent / Sodium bisulfate / H₂O; ethanol

With sodium hydrogen sulfate; sodium acetate; pyridinium chlorochromate; In ethanol; water;

DOI:10.1016/S0040-4039(00)85649-X

Reference yield: 71.0%

potassium cyanide (151-50-8) + Sodium; hydroxy-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanesulfonate (85539-39-5) → Hydroxy-[(1S,5R,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-acetonitrile (85539-40-8)

Guidance literature:

In dichloromethane; water;

DOI:10.1016/S0040-4039(00)85649-X

upstream raw materials:

(1S,5R,7S)-3-(Toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]nonane-7-carbaldehyde

[(1S,5R,7S)-3-(Toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methanol

Downstream raw materials:

Hydroxy-[(1S,5R,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-acetonitrile

Toluene-4-sulfonic acid cyano-[(1R,5S,7S)-3-(toluene-4-sulfonyl)-3-aza-bicyclo[3.3.1]non-7-yl]-methyl ester

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