(S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate

Base Information

• Chemical Name: (S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate
• CAS No.: 1002321-51-8
• Molecular Formula: C₁₉H₂₃NO₆
• Molecular Weight: 361.395

Synonyms:(S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate

Chemical Property of (S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate

Chemical Property:

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Technology Process of (S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate

There total 1 articles about (S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H29NO6Se → (S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate (1002321-51-8)

Guidance literature:

With pyridine; dihydrogen peroxide; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo701968d

Reference yield: 89.0%

(S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate (1002321-51-8) + N-methylmethyleneamine N-oxide (54125-41-6) → (3aS,6R,6aR)-5-tert-butyl 6-methyl 6-[(benzyloxy)methyl]-2-methyl-4-oxohexahydro-5H-pyrrolo[3,4-d]isoxazole-5,6-dicarboxylate + (3aR,6R,6aS)-5-tert-butyl 6-methyl 6-[(benzyloxy)methyl]-2-methyl-4-oxohexahydro-5H-pyrrolo[3,4-d]isoxazole-5,6-dicarboxylate (1002321-59-6)

Guidance literature:

In toluene; at 110 ℃; for 2.2h;

DOI:10.1021/jo701968d

Reference yield:

(S)-1-tert-butyl 2-methyl 2-[(benzyloxy)methyl]-5-oxo-1H-pyrrole-1,2-(2H,5H)-dicarboxylate (1002321-51-8) → (S)-methyl 2-benzyloxymethyl-5-oxo-2,5-dihydro-1H-pyrrole-2-carboxylate

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1021/jo701968d

Downstream raw materials:

(3aR,6R,6aS)-5-tert-butyl 6-methyl 6-[(benzyloxy)methyl]-2-methyl-4-oxohexahydro-5H-pyrrolo[3,4-d]isoxazole-5,6-dicarboxylate

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