5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde

Base Information

Chemical Name:5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde
CAS No.:1564287-92-8
Molecular Formula:C₂₉H₂₇NO₄
Molecular Weight:453.538
Hs Code.:

Synonyms:5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde

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Chemical Property of 5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde

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Technology Process of 5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde

There total 4 articles about 5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1564287-91-7
3-(5-formyl-2-furan)-7-bromo-10-butyl-10H-phenoxazine

: 22237-13-4
(4-ethoxyphenyl)boronic acid

: 1564287-92-8
5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde

Guidance literature:: 3-(5-formyl-2-furan)-7-bromo-10-butyl-10H-phenoxazine; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 0.5h; Reflux;

(4-ethoxyphenyl)boronic acid; In tetrahydrofuran; water; for 15h; Reflux;
DOI:10.1016/j.dyepig.2013.12.022

Reference yield:

: 135-67-1
phenoxazine

: 1564287-92-8
5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 24 h / 20 °C

2.1: N-Bromosuccinimide / chloroform / 20 °C

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 80 °C / Inert atmosphere

4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 0.5 h / Reflux

4.2: 15 h / Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; sodium hydroxide; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide; 3.1: |Suzuki Coupling / 4.1: |Suzuki Coupling / 4.2: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2013.12.022

Reference yield:

: 10-butyl-10H-phenoxazine

: 1564287-92-8
5-(3-(4-ethoxyphenyl)-10-butyl-10H-phenothiazin-7-yl)furan-2-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / chloroform / 20 °C

2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 80 °C / Inert atmosphere

3.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 0.5 h / Reflux

3.2: 15 h / Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; chloroform; water; 2.1: |Suzuki Coupling / 3.1: |Suzuki Coupling / 3.2: |Suzuki Coupling;
DOI:10.1016/j.dyepig.2013.12.022