3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose

Base Information

Chemical Name:3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose
CAS No.:302783-25-1
Molecular Formula:C₂₅H₃₀O₇
Molecular Weight:442.509
Hs Code.:

Synonyms:3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose

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Chemical Property of 3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose

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Technology Process of 3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose

There total 1 articles about 3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 85315-68-0
3-C-(benzyloxymethyl)-3-deoxy-1,2-O-isopropylidene-α-D-allofuranose

: 302783-25-1
3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 55 ℃; for 4h;
DOI:10.1248/cpb.48.1761

Reference yield: 98.0%

: 302783-25-1
3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose

: (R)-1-((3aR,6R,6aR)-6-Benzyloxymethyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanol

Guidance literature:: With tri-n-butyl-tin hydride; magnesium bromide; In dichloromethane; at 20 ℃; for 0.166667h;
DOI:10.1016/S0040-4039(00)01017-0

Reference yield: 56.0%

: 302783-25-1
3-C-benzyloxymethyl-3-deoxy-1,2-O-isopropylidene-5,6-O-(4-methoxybenzylidene)-α-D-allofuranose

: (R)-1-((3aR,6R,6aR)-6-Benzyloxymethyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-ethane-1,2-diol

: (R)-1-((3aR,6R,6aR)-6-Benzyloxymethyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl)-2-(4-methoxy-benzyloxy)-ethanol

Guidance literature:: With tri-n-butyl-tin hydride; zinc(II) chloride; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/S0040-4039(00)01017-0