methyl 3-<<4-phenyl>sulfonyl>propionate

Base Information

Chemical Name:methyl 3-<<4-phenyl>sulfonyl>propionate
CAS No.:130198-93-5
Molecular Formula:C₁₄H₁₉Cl₂NO₄S
Molecular Weight:368.281
Hs Code.:

methyl 3-<<4-<N,N-bis(2-chloroethyl)amino>phenyl>sulfonyl>propionate

Synonyms:methyl 3-<<4-phenyl>sulfonyl>propionate

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Chemical Property of methyl 3-<<4-phenyl>sulfonyl>propionate

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Technology Process of methyl 3-<<4-phenyl>sulfonyl>propionate

There total 8 articles about methyl 3-<<4-phenyl>sulfonyl>propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 130198-90-2
methyl 3-<<4-phenyl>thio>propionate

: 130198-93-5
methyl 3-<<4-phenyl>sulfonyl>propionate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 20h;
DOI:10.1021/jm00173a016

Reference yield:

: 100132-31-8
4-benzenethiol

: 130198-93-5
methyl 3-<<4-phenyl>sulfonyl>propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / K₂CO₃ / methanol / 0.17 h / Heating

2: Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

3: NaCl / dimethylformamide / 0.08 h / 120 °C

4: 84 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / 20 °C

With potassium carbonate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00173a016

Reference yield:

: 130219-46-4
S-<(benzyloxy)carbonyl>-4-aminobenzenethiol

: 130198-93-5
methyl 3-<<4-phenyl>sulfonyl>propionate

Guidance literature:: Multi-step reaction with 6 steps

1: 79 percent / AcOH / tetrahydrofuran / 336 h / 20 °C

2: 56 percent / NaOH / ethanol / 2 h / Heating

3: 57 percent / K₂CO₃ / methanol / 0.17 h / Heating

4: Et₃N / CH₂Cl₂ / 0.75 h / 0 °C

5: NaCl / dimethylformamide / 0.08 h / 120 °C

6: 84 percent / 3-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / 20 °C

With sodium hydroxide; potassium carbonate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium chloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00173a016