anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one

Base Information

Chemical Name:anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one
CAS No.:66953-28-4
Molecular Formula:C₁₀H₁₂O
Molecular Weight:148.205
Hs Code.:

anti-tricyclo<4.2.1.1<sup>2,5</sup>>dec-2-en-9-one

Synonyms:anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one

There total 1 articles about anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 694-28-0
2-chlorocyclopentanone

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 35394-09-3
2-methoxycyclopentanone

: 67009-89-6
syn-Tricyclo<4.2.1.1^2,5>dec-3-en-9-on

: 66953-28-4
anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one

Guidance literature:: With sodium methylate; In methanol; at 0 ℃; for 0.5h;

Reference yield:

: 66953-28-4
anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one

: 1636-39-1
bicyclopentyl

Guidance literature:: Multi-step reaction with 3 steps

1: 25percent KOH, N₂H₄*H₂O / various solvent(s) / 18 h / 120 °C

2: various solvent(s) / 6 h / 150 deg C up to 200 deg C

3: H₂ / Pd/C / diethyl ether / 2 h / Ambient temperature

With potassium hydroxide; hydrogen; hydrazine hydrate; palladium on activated charcoal; In diethyl ether;

Reference yield:

: 66953-28-4
anti-tricyclo<4.2.1.1^2,5>dec-2-en-9-one

: 2825-83-4
(3aR,4R,7S,7aS)-octahydro-1H-4,7-methanoindene

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / Na / toluene; propan-2-ol / 4 h / Heating

2: 93 percent / H₂ / 5percent Pd/C / diethyl ether

3: Et₃SiH, BF₃ / CH₂Cl₂ / 0.08 h / Ambient temperature

With triethylsilane; boron trifluoride; hydrogen; sodium; palladium on activated charcoal; In diethyl ether; dichloromethane; isopropyl alcohol; toluene;
DOI:10.1002/hlca.19880710420