Technology Process of isoanomoian A
There total 6 articles about isoanomoian A which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 0 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/np300102z
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / N,N-dimethyl-formamide / 12 h / 0 - 20 °C / Inert atmosphere
2: water; lithium hydroxide / tetrahydrofuran / 20 °C
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 12 h / 0 °C / Inert atmosphere
With
water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/np300102z
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetone / Reflux; Inert atmosphere
2: trifluoroacetic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 20 °C / Inert atmosphere
4: trifluoroacetic acid / dichloromethane / 12 h / 0 °C / Inert atmosphere
With
potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/np300102z
