N₂-phenethyl-4-[(E)-2-(methylsulfanyl)-1-nitro-2-(phenethylamino)-1-ethenyl]-3-nitro-4H-2-chromenamine

Base Information

• Chemical Name: N₂-phenethyl-4-[(E)-2-(methylsulfanyl)-1-nitro-2-(phenethylamino)-1-ethenyl]-3-nitro-4H-2-chromenamine
• CAS No.: 1173429-82-7
• Molecular Formula: C₂₈H₂₈N₄O₅S
• Molecular Weight: 532.62

Synonyms:N₂-phenethyl-4-[(E)-2-(methylsulfanyl)-1-nitro-2-(phenethylamino)-1-ethenyl]-3-nitro-4H-2-chromenamine

Chemical Property of N₂-phenethyl-4-[(E)-2-(methylsulfanyl)-1-nitro-2-(phenethylamino)-1-ethenyl]-3-nitro-4H-2-chromenamine

Chemical Property:

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Technology Process of N₂-phenethyl-4-[(E)-2-(methylsulfanyl)-1-nitro-2-(phenethylamino)-1-ethenyl]-3-nitro-4H-2-chromenamine

There total 1 articles about N₂-phenethyl-4-[(E)-2-(methylsulfanyl)-1-nitro-2-(phenethylamino)-1-ethenyl]-3-nitro-4H-2-chromenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

salicylaldehyde (90-02-8) + N-[(E)-1-(methylsulfanyl)-2-nitro-1-ethenyl]-N-phenethylamine (102721-77-7) → N-[4-(methylsulfanyl)-3-nitro-4H-2-chromenyl]-N-phenethylamine (1173429-72-5) + N2-phenethyl-4-[(E)-2-(methylsulfanyl)-1-nitro-2-(phenethylamino)-1-ethenyl]-3-nitro-4H-2-chromenamine (1173429-82-7)

Guidance literature:

salicylaldehyde; With sodium hydride; In tetrahydrofuran; for 0.0833333h;

N-[(E)-1-(methylsulfanyl)-2-nitro-1-ethenyl]-N-phenethylamine; In tetrahydrofuran; at 20 ℃; for 17h; Inert atmosphere; Reflux;

DOI:10.1016/j.tetlet.2009.04.018

upstream raw materials:

salicylaldehyde

N-[(E)-1-(methylsulfanyl)-2-nitro-1-ethenyl]-N-phenethylamine

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