C₃₃H₅₈O₂Si₂

Base Information

Chemical Name:C₃₃H₅₈O₂Si₂
CAS No.:1432046-28-0
Molecular Formula:C₃₃H₅₈O₂Si₂
Molecular Weight:542.993
Hs Code.:

C<sub>33</sub>H<sub>58</sub>O<sub>2</sub>Si<sub>2</sub>

Synonyms:C₃₃H₅₈O₂Si₂

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Chemical Property of C₃₃H₅₈O₂Si₂

Chemical Property:

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Technology Process of C₃₃H₅₈O₂Si₂

There total 3 articles about C₃₃H₅₈O₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₅₈O₃Si₂

: 1432046-28-0
C₃₃H₅₈O₂Si₂

Guidance literature:: With ammonia; lithium; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere;
DOI:10.1007/s11426-012-4826-0

Reference yield:

: 564-20-5,1216-84-8,30450-17-0,58976-28-6,64090-92-2,67844-42-2,79768-41-5,79768-42-6,86688-27-9,86688-28-0,95406-08-9,98719-44-9,98719-46-1,131831-65-7,140851-80-5
(3aR)-(+)-sclareolide

: 1432046-28-0
C₃₃H₅₈O₂Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: diethyl ether / 0.25 h / 20 °C / Inert atmosphere

2.1: maleic anhydride; dihydrogen peroxide / dichloromethane; water / 26 h / Inert atmosphere

3.1: potassium hydroxide / methanol / 0.17 h / Inert atmosphere

4.1: oxalyl dichloride; triethylamine; thioacetone / dichloromethane / 1.5 h / -78 - 0 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Reflux

6.1: tert.-butyl lithium / diethyl ether / 0.5 h / -78 °C / Inert atmosphere

6.2: 0.5 h / -78 °C / Inert atmosphere

7.1: ammonia; lithium / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

With maleic anhydride; oxalyl dichloride; thioacetone; ammonia; dihydrogen peroxide; tert.-butyl lithium; lithium; toluene-4-sulfonic acid; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene;
DOI:10.1007/s11426-012-4826-0

Reference yield:

: 19895-03-5
1-((1R,2R,4aS,8aS)-2-hydroxy-2,5,5,8a-tetramethyldecahydronaphthalen-1-yl)propan-2-one

: 1432046-28-0
C₃₃H₅₈O₂Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: maleic anhydride; dihydrogen peroxide / dichloromethane; water / 26 h / Inert atmosphere

2.1: potassium hydroxide / methanol / 0.17 h / Inert atmosphere

3.1: oxalyl dichloride; triethylamine; thioacetone / dichloromethane / 1.5 h / -78 - 0 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Reflux

5.1: tert.-butyl lithium / diethyl ether / 0.5 h / -78 °C / Inert atmosphere

5.2: 0.5 h / -78 °C / Inert atmosphere

6.1: ammonia; lithium / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

With maleic anhydride; oxalyl dichloride; thioacetone; ammonia; dihydrogen peroxide; tert.-butyl lithium; lithium; toluene-4-sulfonic acid; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene;
DOI:10.1007/s11426-012-4826-0