9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether

Base Information

Chemical Name:9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether
CAS No.:80955-85-7
Molecular Formula:C₄₉H₄₂F₃NO₁₂
Molecular Weight:893.867
Hs Code.:

Synonyms:9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether

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Chemical Property of 9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether

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Technology Process of 9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether

There total 1 articles about 9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 68168-15-0
9,10-anhydro-N-(trifluoroacetyl)adriamycin

: 14470-28-1
mono-4-methoxytrityl chloride

: 80955-85-7
9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether

Guidance literature:: With pyridine; at 65 ℃; for 6h;
DOI:10.1021/jm00346a027

Reference yield: 77.0%

: 80955-85-7
9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether

: 80955-86-8
9,10-anhydroadriamycin 14-O-(p-anisyldiphenylmethyl)

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 0 ℃; for 4h;
DOI:10.1021/jm00346a027

Reference yield:

: 80955-85-7
9,10-anhydro-N-(trifluoroacetyl)adriamycin 14-O-(p-anisyldiphenylmethyl) ether

: 80948-70-5
9,10-anhydroadriamycinone

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / aq. 0.1 N NaOH / tetrahydrofuran / 4 h / 0 °C

2: 80percent aq. acetic acid / 3 h / Ambient temperature

With sodium hydroxide; acetic acid; In tetrahydrofuran;
DOI:10.1021/jm00346a027