(1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

Base Information

Chemical Name:(1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol
CAS No.:1310418-46-2
Molecular Formula:C₂₃H₃₆O₃
Molecular Weight:360.537
Hs Code.:

Synonyms:(1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

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Chemical Property of (1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

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Technology Process of (1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

There total 2 articles about (1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 52617-99-9
(+)-drimane-8,11-diol

: 1261826-46-3
1-iodo-3-methoxy-5-methylbenzene

: 1310418-46-2
(1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

Guidance literature:: (+)-drimane-8,11-diol; With 3,4,7,8-Tetramethyl-o-phenanthrolin; copper(l) iodide; for 0.25h; Sealed tube; Inert atmosphere;

1-iodo-3-methoxy-5-methylbenzene; In diethylene glycol dimethyl ether; toluene; at 20 - 120 ℃; for 18h; Inert atmosphere;

Reference yield:

: 29578-83-4
3-bromo-5-methoxytoluene

: 1310418-46-2
(1S,2R,4aS,8aS)-1-(3-methoxy-5-methylphenoxymethyl)-2,5,5,8a-tetramethyldecahydronaphthalen-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium iodide; N,N`-dimethylethylenediamine / copper(l) iodide / 1,4-dioxane / 18 h / 20 - 110 °C / Sealed tube; Inert atmosphere

2.1: 3,4,7,8-Tetramethyl-o-phenanthrolin / copper(l) iodide / 0.25 h / Sealed tube; Inert atmosphere

2.2: 18 h / 20 - 120 °C / Inert atmosphere

With 3,4,7,8-Tetramethyl-o-phenanthrolin; sodium iodide; N,N`-dimethylethylenediamine; copper(l) iodide; In 1,4-dioxane;