3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Base Information

Chemical Name:3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one
CAS No.:1229516-39-5
Molecular Formula:C₃₀H₂₆O₄
Molecular Weight:453.501
Hs Code.:

3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-<sup>(13)</sup>C<sub>3</sub>]propen-1-one

Synonyms:3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

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Chemical Property of 3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

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Technology Process of 3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

There total 5 articles about 3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1229516-29-3
2,4-[1',2'-⁽¹³⁾C₂]dibenzyloxyacetophenone

: 95537-93-2
α-[¹³C]-4-methoxybenzaldehyde

: 1229516-39-5
3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; for 6h; Inert atmosphere; Reflux;
DOI:10.1002/jlcr.1732

Reference yield:

: 1333245-00-3
(¹³C)-4-methoxybenzonitrile

: 1229516-39-5
3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran / 20 °C

2: potassium hydroxide / tetrahydrofuran; methanol / 6 h / Inert atmosphere; Reflux

With diisobutylaluminium hydride; potassium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1002/jlcr.1732

Reference yield:

: 696-62-8
para-iodoanisole

: 1229516-39-5
3-(4-methoxyphenyl)-1-[2,4-bis(benzyloxy)phenyl]-2-[1,2,3-⁽¹³⁾C₃]propen-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; calcium hydroxide / N,N-dimethyl-formamide / 16 h / Reflux

2: diisobutylaluminium hydride / tetrahydrofuran / 20 °C

3: potassium hydroxide / tetrahydrofuran; methanol / 6 h / Inert atmosphere; Reflux

With palladium diacetate; diisobutylaluminium hydride; potassium hydroxide; calcium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.1732