C₂₃H₃₃BrOS

Base Information

• Chemical Name: C₂₃H₃₃BrOS
• CAS No.: 1246922-04-2
• Molecular Formula: C₂₃H₃₃BrOS
• Molecular Weight: 437.484
• Mol file: 1246922-04-2.mol

Synonyms:C₂₃H₃₃BrOS

Chemical Property of C₂₃H₃₃BrOS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₂₃H₃₃BrOS

There total 1 articles about C₂₃H₃₃BrOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H34OS (1246922-06-4) → C23H33BrOS (1246922-04-2)

Guidance literature:

With N-Bromosuccinimide; In tetrahydrofuran; at 0 - 5 ℃; for 15h;

DOI:10.1002/anie.200903247

Reference yield: 30.0%

5-(4-methoxylphenyl)-2-bromothiophene (54095-24-8) + C23H33BrOS (1246922-04-2) → 4-dodecyl-5,5'-bis(4-methoxyphenyl)-2,2'-bithiophene

Guidance literature:

5-(4-methoxylphenyl)-2-bromothiophene; With magnesium; In tetrahydrofuran; Reflux;

C₂₃H₃₃BrOS; With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); In tetrahydrofuran; at 0 ℃; Reflux;

DOI:10.1002/anie.200903247

Reference yield:

C23H33BrOS (1246922-04-2) → C22H31BrOS

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c8tc04890h

upstream raw materials:

C₂₃H₃₄OS