Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid

Base Information

Chemical Name:Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid
CAS No.:127977-03-1
Molecular Formula:C₁₈H₂₅N₃O₇S
Molecular Weight:427.478
Hs Code.:

Synonyms:Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid

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Chemical Property of Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid

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Technology Process of Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid

There total 5 articles about Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127953-58-6
Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid allyl ester

: 127977-03-1
Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid

Guidance literature:: With sodium hydroxide; In ethanol; Ambient temperature;
DOI:10.1021/jm00084a008

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 127977-03-1
Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 43 percent / 3.33 N aq. NaOH / tetrahydrofuran / 6 h / Ambient temperature

2: 1.) 1,1'-carbonyldiimidazole, 2.) NH₃ gas / 1.) CH₂Cl₂, THF, 45 min, 2.) CH₂Cl₂, THF, RT, overnight

3: 72.3 percent / acetone / 48 h / Heating

4: conc. aq. H₂SO₄ / Ambient temperature

5: 1 N aq. NaOH / ethanol / Ambient temperature

With sodium hydroxide; sulfuric acid; ammonia; 1,1'-carbonyldiimidazole; In tetrahydrofuran; ethanol; acetone;
DOI:10.1021/jm00084a008

Reference yield:

: 124278-39-3
N-(4-MorpholinYlsulfonyl)-L-phenylalanine

: 127977-03-1
Allyloxy-[(S)-2-(morpholine-4-sulfonylamino)-3-phenyl-propionylamino]-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 1,1'-carbonyldiimidazole, 2.) NH₃ gas / 1.) CH₂Cl₂, THF, 45 min, 2.) CH₂Cl₂, THF, RT, overnight

2: 72.3 percent / acetone / 48 h / Heating

3: conc. aq. H₂SO₄ / Ambient temperature

4: 1 N aq. NaOH / ethanol / Ambient temperature

With sodium hydroxide; sulfuric acid; ammonia; 1,1'-carbonyldiimidazole; In ethanol; acetone;
DOI:10.1021/jm00084a008