12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline

Base Information

• Chemical Name: 12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline
• CAS No.: 161769-18-2
• Molecular Formula: C₃₀H₂₉N₃
• Molecular Weight: 431.58

Synonyms:12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline

Chemical Property of 12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline

Chemical Property:

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Technology Process of 12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline

There total 1 articles about 12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-Aminonicotinaldehyde (7521-41-7) + 5-benzylidene-9-n-butyl-2,3,5,6,7,8-hexahydro-4(1H)-acridinone (105282-71-1) → 12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline (161769-18-2)

Guidance literature:

With potassium hydroxide; In methanol; for 24h; Heating;

DOI:10.1016/0040-4020(94)00902-7

Reference yield:

12-benzylidene-8-n-butyl-6,7,9,10,11,12-hexahydrobenzopyrido<3,2-j><1,10>phenanthroline (161769-18-2) → 8-n-butyl-6,7,10,11-tetrahydrobenzopyrido<3,2-j><1,10>phenanthrolin-12(9H)-one dinitrophenylhydrazone

Guidance literature:

Multi-step reaction with 2 steps

1: 1) ozone, 2) Me₂S / 1) CH₂Cl₂, MeOH, -78 deg C, 2) CH₂Cl₂, MeOH, -78 deg C to Rt, overnight

2: 75 percent / CH₂Cl₂; ethanol / 36 h / Ambient temperature

With dimethylsulfide; ozone; In ethanol; dichloromethane;

DOI:10.1016/0040-4020(94)00902-7

upstream raw materials:

2-Aminonicotinaldehyde

5-benzylidene-9-n-butyl-2,3,5,6,7,8-hexahydro-4(1H)-acridinone

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