C₃₂H₃₆N₄O₁₈

Base Information

Chemical Name:C₃₂H₃₆N₄O₁₈
CAS No.:1365254-67-6
Molecular Formula:C₃₂H₃₆N₄O₁₈
Molecular Weight:764.654
Hs Code.:

C<sub>32</sub>H<sub>36</sub>N<sub>4</sub>O<sub>18</sub>

Synonyms:C₃₂H₃₆N₄O₁₈

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Chemical Property of C₃₂H₃₆N₄O₁₈

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Technology Process of C₃₂H₃₆N₄O₁₈

There total 5 articles about C₃₂H₃₆N₄O₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: C₄₆H₄₈N₄O₁₈

: 1365254-67-6
C₃₂H₃₆N₄O₁₈

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2012.01.080

Reference yield:

: 1365254-70-1
C₂₆H₃₈N₂O₁₂

: 1365254-67-6
C₃₂H₃₆N₄O₁₈

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / water; ethyl acetate / 10 h / 20 °C / Inert atmosphere

2: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere

3: osmium(VIII) oxide; 4-methylmorpholine N-oxide; hydroquinidein 1,4-phthalazinediyl diether / tetrahydrofuran; water; tert-butyl alcohol / 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; osmium(VIII) oxide; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinidein 1,4-phthalazinediyl diether; In tetrahydrofuran; methanol; water; ethyl acetate; tert-butyl alcohol; 3: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tet.2012.01.080

Reference yield:

: C₁₆H₂₂N₂O₈*2ClH

: 1365254-67-6
C₃₂H₃₆N₄O₁₈

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere

2: osmium(VIII) oxide; 4-methylmorpholine N-oxide; hydroquinidein 1,4-phthalazinediyl diether / tetrahydrofuran; water; tert-butyl alcohol / 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C

With 4-methyl-morpholine; osmium(VIII) oxide; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinidein 1,4-phthalazinediyl diether; In tetrahydrofuran; methanol; water; tert-butyl alcohol; 2: Sharpless asymmetric dihydroxylation;
DOI:10.1016/j.tet.2012.01.080