C₁₉H₂₈O₆

Base Information

Chemical Name:C₁₉H₂₈O₆
CAS No.:952492-26-1
Molecular Formula:C₁₉H₂₈O₆
Molecular Weight:352.428
Hs Code.:

C<sub>19</sub>H<sub>28</sub>O<sub>6</sub>

Synonyms:C₁₉H₂₈O₆

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Chemical Property of C₁₉H₂₈O₆

Chemical Property:

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Technology Process of C₁₉H₂₈O₆

There total 18 articles about C₁₉H₂₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₈O₅

: 952492-26-1
C₁₉H₂₈O₆

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate; 4A MS; In dichloromethane; at -20 ℃; for 8h;
DOI:10.1016/j.tetlet.2007.07.068

Reference yield:

: 952492-20-5
C₂₆H₄₄O₄Si

: 952492-26-1
C₁₉H₂₈O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: 91 percent / OsO₄; NMO / acetone; H₂O / 72 h / 20 °C

2.1: 2,6-lutidine / CH₂Cl₂ / 0.08 h / 0 °C

3.1: DIBAL-H / CH₂Cl₂ / 0.33 h / -78 °C

4.1: MsCl; Et₃N; DMAP / CH₂Cl₂ / 0.25 h / 0 °C

4.2: 52 percent / K₂CO₃ / methanol / 18 h / 20 °C

5.1: CSA / CH₂Cl₂; methanol / 6 h / 0 °C

6.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 °C

7.1: CH₂Cl₂ / 72 h / 20 °C

8.1: DIBAL-H / CH₂Cl₂ / 0.25 h / -78 °C

9.1: TBAF / tetrahydrofuran / 6 h / 0 - 20 °C

10.1: Ti(OiPr)4; (+)-DIPT; TBHP / 4A MS / CH₂Cl₂ / 8 h / -20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; oxalyl dichloride; L-(+)-diisopropyl tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; 4A MS; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 10.1: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2007.07.068

Reference yield:

: C₃₂H₆₀O₆Si₂

: 952492-26-1
C₁₉H₂₈O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: DIBAL-H / CH₂Cl₂ / 0.33 h / -78 °C

2.1: MsCl; Et₃N; DMAP / CH₂Cl₂ / 0.25 h / 0 °C

2.2: 52 percent / K₂CO₃ / methanol / 18 h / 20 °C

3.1: CSA / CH₂Cl₂; methanol / 6 h / 0 °C

4.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 °C

5.1: CH₂Cl₂ / 72 h / 20 °C

6.1: DIBAL-H / CH₂Cl₂ / 0.25 h / -78 °C

7.1: TBAF / tetrahydrofuran / 6 h / 0 - 20 °C

8.1: Ti(OiPr)4; (+)-DIPT; TBHP / 4A MS / CH₂Cl₂ / 8 h / -20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; oxalyl dichloride; L-(+)-diisopropyl tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; 4A MS; In tetrahydrofuran; methanol; dichloromethane; 8.1: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2007.07.068