N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid

Base Information

Chemical Name:N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid
CAS No.:99744-70-4
Molecular Formula:C₄₀H₄₀N₂O₅P*Cl
Molecular Weight:695.195
Hs Code.:

Synonyms:N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid

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Chemical Property of N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid

Chemical Property:

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Technology Process of N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid

There total 6 articles about N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 99744-62-4
N-<2-(Triphenylphosphonio)isopropyloxy>-L-phenylalanyl-L-phenylalanin-tert-butylester-chlorid

: 99744-70-4
N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid

Guidance literature:: With hydrogenchloride; In dichloromethane; at -70 ℃; for 0.5h;

Reference yield:

: 16874-17-2
L-phenylalanine tert-butyl ester

: 99744-70-4
N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / EEDQ / CHCl₃ / 15 h / Ambient temperature

2: 99 percent / HCl / CH₂Cl₂ / 0.5 h / -70 °C

With hydrogenchloride; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; chloroform;

Reference yield:

: 36466-73-6
(2-Hydroxypropyl)triphenylphosphonium-chlorid

: 99744-70-4
N-<2-(Triphenylphosphonio)isopropyloxycarbonyl>-L-phenylalanyl-L-phenylalanin-chlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / CHCl₃ / 5 h / -15 °C

2: 57 percent / CHCl₃ / 12 h / Ambient temperature

3: 92 percent / EEDQ / CHCl₃ / 15 h / Ambient temperature

4: 99 percent / HCl / CH₂Cl₂ / 0.5 h / -70 °C

With hydrogenchloride; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In dichloromethane; chloroform;