1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol

Base Information

Chemical Name:1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol
CAS No.:131389-40-7
Molecular Formula:C₄₀H₄₆O₇Si
Molecular Weight:666.887
Hs Code.:

Synonyms:1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol

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Chemical Property of 1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol

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Technology Process of 1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol

There total 1 articles about 1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 67093-26-9
2-bromo-1-(hydroxymethyl)-3,5-bis-(benzyloxy)-benzene

: 142393-21-3,130912-41-3
1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-tributylstannyl-D-arabino-hex-1-enitol

: 131389-40-7
1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol

: 131414-13-6
1,1'-bis(1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-D-arabino-hex-1-enitol)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In toluene; for 3h; Heating;
DOI:10.1016/S0040-4039(00)97832-8

Reference yield: 12.0%

: 131389-40-7
1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol

: 131389-41-8,131485-58-0
1,1²-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-α-D-glucopyranose

: 131389-41-8,131485-58-0
1,1²-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-β-D-glucopyranose

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 5h;
DOI:10.1016/S0040-4039(00)97832-8

Reference yield:

: 131389-40-7
1,5-anhydro-4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-2-deoxy-1-(4,6-dibenzyloxy-2-hydroxymethylphenyl)-D-arabino-hex-1-enitol

: 131389-45-2
2-(4,6-O-benzylidene-3-O-tert-butyldimethylsilyl-β-D-glucopyranosyl)-3,5-dibenzyloxy-1-hydroxymethylbenzene

Guidance literature:: With sodium hydroxide; borane-THF; dihydrogen peroxide; Yield given. Multistep reaction; 1) RT, 1 h;
DOI:10.1016/S0040-4039(00)97832-8