2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene

Base Information

• Chemical Name: 2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene
• CAS No.: 1375353-29-9
• Molecular Formula: C₆₀H₁₀₀O₁₀Si₆
• Molecular Weight: 1149.96

Synonyms:2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene

Chemical Property of 2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene

Chemical Property:

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Technology Process of 2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene

There total 1 articles about 2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

2,7-Dihydroxynaphthalene (582-17-2) + C31H51N4O7PolSSi3 → 2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene (1375353-29-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm2016045

Reference yield: 55.0%

2,7-bis[(3,4,5-tris(tert-butyldimethylsilyloxy)benzoyl)oxy]naphthalene (1375353-29-9) → naphthalene-2,7-diyl bis(3,4,5-trihydroxybenzoate) (1375353-17-5)

Guidance literature:

With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm2016045

upstream raw materials:

2,7-Dihydroxynaphthalene

Downstream raw materials:

naphthalene-2,7-diyl bis(3,4,5-trihydroxybenzoate)

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