Technology Process of 3-Hydroxy-2-benzyliden-2,3-dihydro-benzofuran
There total 1 articles about 3-Hydroxy-2-benzyliden-2,3-dihydro-benzofuran which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
silver carbonate;
In
dimethyl sulfoxide;
at 80 ℃;
for 2h;
Reagent/catalyst;
Solvent;
Temperature;
DOI:10.1039/c6ob00191b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trimethylsilylazide / dimethyl sulfoxide / 80 °C
2: copper(l) iodide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trimethylsilylazide / acetonitrile / 8 h / 80 °C / Molecular sieve; Inert atmosphere
With
copper(l) iodide; trimethylsilylazide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dimethyl sulfoxide; acetonitrile;
DOI:10.1039/c6ob00191b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trimethylsilylazide / dimethyl sulfoxide / 80 °C
2: triphenylphosphine / water; tetrahydrofuran / 20 °C / Inert atmosphere
With
trimethylsilylazide; triphenylphosphine;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1039/c6ob00191b
