(S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate

Base Information

Chemical Name:(S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate
CAS No.:1608150-81-7
Molecular Formula:C₂₅H₄₀N₂O₅
Molecular Weight:448.603
Hs Code.:

Synonyms:(S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate

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Chemical Property of (S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate

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Technology Process of (S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate

There total 2 articles about (S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 2900-27-8
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid

: 29833-32-7
11-aminoundecanoic acid methyl ester hydrochloride

: 1608150-81-7
(S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate

Guidance literature:: (2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.25h; Inert atmosphere;

11-aminoundecanoic acid methyl ester hydrochloride; In dichloromethane; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1039/c4ob00207e

Reference yield:

: 2432-99-7,25587-80-8,84029-94-7
11-aminoundecanoic acid

: 1608150-81-7
(S)-methyl 11-(2-((tert-butoxycarbonyl)amino)-2-phenylacetamido)undecanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 4 h / 20 - 80 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / dichloromethane / 0.25 h / 0 °C / Inert atmosphere

2.2: 18 h / 20 °C / Inert atmosphere

With thionyl chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/c4ob00207e