(3,5-bis(trifluoromethyl)phenyl)lithium

Base Information

Chemical Name:(3,5-bis(trifluoromethyl)phenyl)lithium
CAS No.:107337-73-5
Molecular Formula:C₈H₃F₆Li
Molecular Weight:220.043
Hs Code.:

Synonyms:(3,5-bis(trifluoromethyl)phenyl)lithium

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Chemical Property of (3,5-bis(trifluoromethyl)phenyl)lithium

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Technology Process of (3,5-bis(trifluoromethyl)phenyl)lithium

There total 1 articles about (3,5-bis(trifluoromethyl)phenyl)lithium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 328-70-1
3,6-bis(trifluoromethyl)bromobenzene

: 107337-73-5
(3,5-bis(trifluoromethyl)phenyl)lithium

Guidance literature:: With p-tolyllithium; In tetrahydrofuran; at -70 ℃; for 2h;

Reference yield: 76.0%

: 596093-89-9
12-chloro-5,6,7,12-tetrahydrodibenzo[c,f][1,5]azabismocine

: 107337-73-5
(3,5-bis(trifluoromethyl)phenyl)lithium

: 596093-84-4
[(t)BuN(CH₂C₆H₄)2Bi(3,5-(CF₃)2C₆H₃)]

Guidance literature:: In diethyl ether; a soln. of 3,5-(CF3)2C6H3Li added to a soln. of Bi compd. at -80°C, stirred overnight with gradual warming to room temp.; evapd. (vac.), extd. (CH2Cl2), filtered through Celite which was washed with toluene, the combined filtrate concd. (vac.), decanted, washed (hexane), dried (vac.); another crop obtained from the supernatant by concn.(vac.); elem. anal.;
DOI:10.1016/j.jorganchem.2004.06.041

Reference yield: 69.0%

: diferrocenylmethanone

: 107337-73-5
(3,5-bis(trifluoromethyl)phenyl)lithium

: C₂₉H₂₂F₆Fe₂O

Guidance literature:: diferrocenylmethanone; (3,5-bis(trifluoromethyl)phenyl)lithium; In tetrahydrofuran; at -78 - 20 ℃; for 12h;

for 4h; Reflux;
DOI:10.1039/d1dt03009d