5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

Base Information

Chemical Name:5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate
CAS No.:228562-28-5
Molecular Formula:C₂₇H₂₇ClN₂O₆
Molecular Weight:510.974
Hs Code.:

Synonyms:5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

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Chemical Property of 5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

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Technology Process of 5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

There total 5 articles about 5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: C₂₀H₁₉ClO₅

: 193539-61-6
(Z)-3-Amino-but-2-enoic acid 2-cyano-ethyl ester

: 228562-28-5
5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: In isopropyl alcohol; at 70 - 120 ℃; for 4h;

Reference yield:

: 6956-50-9
ethyl 4,4-dimethoxy-3-oxo-butyrate

: 228562-28-5
5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / toluene / 72 h / Heating / reflux

2: piperidine / benzene / Heating / reflux

3: isopropyl alcohol / 4 h / 70 - 120 °C

With dmap; piperidine; In isopropyl alcohol; toluene; benzene;

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 228562-28-5
5-(2-cyanoethyl) 3-benzyl 4-(3-chlorophenyl)-2-dimethoxymethyl-6-methyl-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: dmap / toluene / 72 h / Heating / reflux

2: piperidine / benzene / Heating / reflux

3: isopropyl alcohol / 4 h / 70 - 120 °C

With dmap; piperidine; In isopropyl alcohol; toluene; benzene;