(+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate

Base Information

Chemical Name:(+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate
CAS No.:121893-30-9
Molecular Formula:C₁₈H₂₆O₂Si
Molecular Weight:302.489
Hs Code.:

Synonyms:(+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate

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Chemical Property of (+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate

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Technology Process of (+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate

There total 2 articles about (+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121893-28-5
(+/-)-2-methyl-1-cyclopentene-1,3-dimethanol

: 121893-30-9
(+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / pyridine / tetrahydrofuran / 14 h / Ambient temperature

2: 94 percent / tetrahydrofuran / 12 h / -60 °C

With pyridine; In tetrahydrofuran;
DOI:10.1016/S0040-4020(01)86640-0

Reference yield:

: 121893-27-4
2-Methyl-cyclopent-1-ene-1,3-dicarboxylic acid dimethyl ester

: 121893-30-9
(+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / lithium aluminum hydride / diethyl ether / 14.5 h / -78 - 20 °C

2: 85 percent / pyridine / tetrahydrofuran / 14 h / Ambient temperature

3: 94 percent / tetrahydrofuran / 12 h / -60 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)86640-0

Reference yield: 87.0%

: 121893-30-9
(+/-)-3-<(dimethylphenylsilyl)methyl>-2-methyl-2-cyclopentene-1-methanol acetate

: 121893-31-0
(+/-)-3-<(dimethylphenylsilyl)methyl>-2-cyclopentene-1-methanol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; 1) -45 deg C, 1 h, 2) -45 deg C - room temperature, 3 h;
DOI:10.1016/S0040-4020(01)86640-0