Spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one, 2'-[(2-chlorophenyl)amino]-6'-(diethylamino)-

Base Information

Chemical Name:Spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one, 2'-[(2-chlorophenyl)amino]-6'-(diethylamino)-
CAS No.:68506-98-9
Molecular Formula:C30H25ClN2O3
Molecular Weight:496.993
Hs Code.:
European Community (EC) Number:270-930-1,276-628-6
DSSTox Substance ID:DTXSID30887427
Nikkaji Number:J278.541B
Mol file:68506-98-9.mol

Synonyms:68506-98-9;C30H25ClN2O3;Spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one, 2'-[(2-chlorophenyl)amino]-6'-(diethylamino)-;EINECS 276-628-6;2'-[(2-chlorophenyl)amino]-6'-(diethylamino)spiro[isobenzofuran-1(3H),9'-[9H]xanthene]-3-one;EINECS 270-930-1;2'-(2-chloroanilino)-6'-(diethylamino)spiro[2-benzofuran-3,9'-xanthene]-1-one;72389-79-8;2'-((Chlorophenyl)amino)-6'-(diethylamino)spiro(isobenzofuran-1(3H),9'-(9H)xanthene)-3-one;3-N,N-Diethylamino-7-(orthochloro)anilinofluoran;C30-H25-Cl-N2-O3;Spiro(isobenzofuran-1(3H),9'-(9H)xanthen)-3-one, 2'-((2-chlorophenyl)amino)-6'-(diethylamino)-;Fluoran Black;2'-((2-Chlorophenyl)amino)-6'-(diethylamino)spiro(isobenzofuran-1(3H),9'-(9H)xanthene)-3-one;2'-[(CHLOROPHENYL)AMINO]-6'-(DIETHYLAMINO)SPIRO[ISOBENZOFURAN-1(3H),9'-[9H]XANTHENE]-3-ONE;2'-[(2-chlorophenyl)amino]-6'-(diethylamino)-3h-spiro[2-benzofuran-1,9'-xanthen]-3-one;2'-(2-Chlorophenylamino)-6'-diethylaminofluoran;SCHEMBL6405302;DTXSID30887427;STL335078;AKOS022107171

Suppliers and Price of Spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one, 2'-[(2-chlorophenyl)amino]-6'-(diethylamino)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 7 raw suppliers

Chemical Property of Spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one, 2'-[(2-chlorophenyl)amino]-6'-(diethylamino)-

Chemical Property:

Boiling Point:672.4oC at 760 mmHg
Flash Point:360.5oC
PSA：50.80000
Density:1.37g/cm3
LogP:7.57080
XLogP3:7.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:496.1553704
Heavy Atom Count:36
Complexity:792

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C1=CC2=C(C=C1)C3(C4=CC=CC=C4C(=O)O3)C5=C(O2)C=CC(=C5)NC6=CC=CC=C6Cl

Technology Process of Spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one, 2'-[(2-chlorophenyl)amino]-6'-(diethylamino)-

There total 9 articles about Spiro[isobenzofuran-1(3H),9'-[9H]xanthen]-3-one, 2'-[(2-chlorophenyl)amino]-6'-(diethylamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.6%

: C₃₂H₂₇ClN₂O₄

: 68506-98-9
N-(4-hydroxyphenyl)stearamide 3-diethylamino-7-(2-chlorophenyl)aminofluoran

Guidance literature:: With water; potassium hydroxide; at 35 ℃; for 3h;

Reference yield:

: C₂₈H₁₉ClN₂O₄

: 68506-98-9
N-(4-hydroxyphenyl)stearamide 3-diethylamino-7-(2-chlorophenyl)aminofluoran

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / toluene / 9.25 h / 20 - 150 °C / 2250.23 Torr / Inert atmosphere

2: potassium hydroxide; water / 3 h / 35 °C

With water; sodium carbonate; potassium hydroxide; In toluene;

Reference yield:

: 554-84-7
meta-nitrophenol

: 68506-98-9
N-(4-hydroxyphenyl)stearamide 3-diethylamino-7-(2-chlorophenyl)aminofluoran

Guidance literature:: Multi-step reaction with 5 steps

1: 5,5-dimethyl-1,3-cyclohexadiene / 130 °C / Inert atmosphere

2: sulfuric acid / 16 h / 0 - 65 °C / Inert atmosphere

3: palladium on activated charcoal; hydrogen / ethanol / 10 - 20 °C / 225.02 - 375.04 Torr

4: sodium carbonate / toluene / 9.25 h / 20 - 150 °C / 2250.23 Torr / Inert atmosphere

5: potassium hydroxide; water / 3 h / 35 °C

With sulfuric acid; palladium on activated charcoal; water; hydrogen; sodium carbonate; potassium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; toluene;