Technology Process of C36H28N10O4
There total 6 articles about C36H28N10O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
water; N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
DOI:10.1021/jm301757v
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydrogen sulfate / N,N-dimethyl acetamide / 12 h / 145 °C
2: pyridine / dichloromethane / 2 h / 20 °C
3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C
4: lithium hydroxide monohydrate / tetrahydrofuran / 20 °C
5: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / 12 h / 20 °C
With
pyridine; sodium hydrogen sulfate; copper(ll) sulfate pentahydrate; lithium hydroxide monohydrate; potassium carbonate; sodium L-ascorbate;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;
DOI:10.1021/jm301757v
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 2 h / 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 20 °C
3: lithium hydroxide monohydrate / tetrahydrofuran / 20 °C
4: sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / 12 h / 20 °C
With
pyridine; copper(ll) sulfate pentahydrate; lithium hydroxide monohydrate; potassium carbonate; sodium L-ascorbate;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm301757v
