DI-N-HEXYL SODIUM SULFOSUCCINATE

Base Information

• Chemical Name: DI-N-HEXYL SODIUM SULFOSUCCINATE
• CAS No.: 3006-15-3
• Molecular Formula: C16H29NaO7S
• Molecular Weight: 388.458
• Hs Code.: 2917 19 80
• Mol file: 3006-15-3.mol

Synonyms:Butanedioicacid, sulfo-, 1,4-dihexyl ester, sodium salt (9CI);Succinic acid, sulfo-, 1,4-dihexylester, sodium salt (8CI);Succinic acid, sulfo-, dihexyl ester, S-sodium salt(7CI);Colawet MA 80;Di-n-hexyl sulfosuccinate sodium salt;Dihexyl ester ofsodium sulfosuccinate;Dihexyl sodiosulfosuccinate;Dihexyl sodiumsulfosuccinate;Dihexyl sulfosuccinate sodium salt;Gemtex 680;Hydropalat 680;MA 80I;Monawet MM 80;SV 1017;Sodiumbis(1-hexyl) sulfosuccinate;Sodium dihexyl sulfosuccinate;Sodiumsulfosuccinic acid dihexyl ester;Sulfobutanedioic acid 1,4-dihexyl estersodium salt;

Chemical Property of DI-N-HEXYL SODIUM SULFOSUCCINATE

Chemical Property:

• Melting Point: 230°C decomposes
• Refractive Index: n20/D 1.435
• PSA: 118.18000
• Density: 1.121 g/mL at 20 °C
• LogP: 3.61810
• Storage Temp.: Store at +15°C to +25°C.
• Solubility.: 364g/l

Purity/Quality:

98%,99%, ^*data from raw suppliers

Dihexyl sodium sulfosuccinate for synthesis. CAS 3006-15-3, pH 5 - 7 (50 g/l, H O, 25 °C)., for synthesis ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22-36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DI-N-HEXYL SODIUM SULFOSUCCINATE

There total 5 articles about DI-N-HEXYL SODIUM SULFOSUCCINATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.7%

maleic acid dihexyl ester (16064-83-8) → sodium 1,4-dihexyl sulfosuccinate (3006-15-3)

Guidance literature:

With sodium hydrogensulfite; In ethanol; at 119.85 ℃;

DOI:10.1021/je060152v

Reference yield:

hexan-1-ol (111-27-3) → sodium 1,4-dihexyl sulfosuccinate (3006-15-3)

Guidance literature:

Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / Heating

2: aq. NaHSO₃ / ethanol / Heating

With sodium hydrogensulfite; toluene-4-sulfonic acid; In ethanol;

DOI:10.1021/je0601659

Reference yield:

hexan-1-ol (111-27-3) → sodium 1,4-dihexyl sulfosuccinate (3006-15-3)

Guidance literature:

Multi-step reaction with 2 steps

1: conc. H₂SO₄ / benzene / 4 h / 54.85 °C

2: sodium hydrogensulfite / H₂O / 99.85 °C

With sulfuric acid; sodium hydrogensulfite; In water; benzene; 1: Esterification / 2: sulfonation;

DOI:10.1039/a904815d

upstream raw materials:

maleic acid dihexyl ester

di-n-hexyl succinate

hexan-1-ol

Downstream raw materials:

Sulfobernsteinsaeure-dihexylester

Refernces

• 1、 Liu, Zhao-Tie,Liu, Ling,Wu, Jin,Song, Liping,Gao, Ziwei,Dong, Wensheng,Lu, Jian. "Solubility and phase behaviors of AOT analogue surfactants in 1,1,1,2-tetrafluoroethane and supercritical carbon dioxide". . p. 2045 - 2050. Retrieved 2007/10/03.
• 2、 Nagasoe, Yasuyuki,Ichiyanagi, Naoki,Okabayashi, Hirofumi,Nave, Sandrine,Eastoe, Julian,O'Connor, Charmian J.. "Raman and IR spectroscopic studies of the interaction between counterion and polar group in self-assembled systems of AOT-homologous 'sodium dialkyl sulfosuccinates'". . p. 4395 - 4407. Retrieved 2007/10/03.