Technology Process of C53H84N4O15*ClH
There total 9 articles about C53H84N4O15*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C
2: triethylamine hydrofluoride / tetrahydrofuran / 12 h / 20 °C
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 20 °C
4: dichloromethane / 1 h / 20 °C
5: ammonium chloride
With
dmap; ammonium chloride; triethylamine hydrofluoride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2012.06.044
- Guidance literature:
-
Multi-step reaction with 7 steps
1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C / 760.05 Torr
3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 12 h / 20 °C
4: triethylamine hydrofluoride / tetrahydrofuran / 12 h / 20 °C
5: dmap; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 20 °C
6: dichloromethane / 1 h / 20 °C
7: ammonium chloride
With
dmap; palladium 10% on activated carbon; hydrogen; ammonium chloride; triethylamine hydrofluoride; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; ethyl acetate;
DOI:10.1016/j.ejmech.2012.06.044