(E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane

Base Information

Chemical Name:(E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane
CAS No.:1379810-81-7
Molecular Formula:C₁₉H₃₁BrO₃Si
Molecular Weight:415.443
Hs Code.:

Synonyms:(E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane

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Chemical Property of (E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane

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Technology Process of (E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane

There total 4 articles about (E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₇BrO₂Si

: 107-30-2
chloromethyl methyl ether

: 1379810-81-7
(E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmcl.2014.04.012

Reference yield:

: 1838-94-4
isoprene epoxide

: 1379810-81-7
(E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane

Guidance literature:: Multi-step reaction with 4 steps

1.1: titanium tetrachloride / dichloromethane / 3.5 h / -78 °C / Inert atmosphere

2.1: 1H-imidazole; dmap / 1 h

3.1: sodium hydride / toluene / 0.58 h / Inert atmosphere

3.2: 19.5 h / 35 °C / Inert atmosphere

4.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

With 1H-imidazole; dmap; titanium tetrachloride; sodium hydride; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2014.04.012

Reference yield:

: 270258-26-9
(E)-tert-butyl(4-chloro-2-methylbut-2-en-1-yloxy)dimethylsilane

: 1379810-81-7
(E)-(4-(5-bromo-2-(methoxymethoxy)phenyl)-2-methylbut-2-enyloxy)(tert-butyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / toluene / 0.58 h / Inert atmosphere

1.2: 19.5 h / 35 °C / Inert atmosphere

2.1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 0 °C / Inert atmosphere

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2014.04.012