3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one

Base Information

Chemical Name:3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one
CAS No.:1012879-41-2
Molecular Formula:C₁₇H₁₇ClN₄O
Molecular Weight:328.801
Hs Code.:

Synonyms:3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one

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Technology Process of 3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one

There total 10 articles about 3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 409082-02-6
ethyl 2-(5-amino-2-chlorophenyl)acetate

: 959163-01-0
6-chloro-4-ethylamino-pyridine-3-carbaldehyde

: 702-24-9
4-methoxy-N-methylbenzylamine

: 1012879-41-2
3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one

Guidance literature:: With caesium carbonate; trifluoroacetic acid;

Reference yield:

: 37777-70-1
2-(2-chloro-5-nitrophenyl)acetic acid

: 1012879-41-2
3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 0 °C / Reflux

2: hydrogenchloride; iron / water; ethanol / 2 h / 50 °C / Reflux

3: trifluoroacetic acid; caesium carbonate

With hydrogenchloride; thionyl chloride; iron; caesium carbonate; trifluoroacetic acid; In ethanol; water;

Reference yield:

: 409082-01-5
ethyl 2-(2-chloro-5-nitrophenyl)acetate

: 1012879-41-2
3-(5-amino-2-chlorophenyl)-1-ethyl-7-(methylamino)-1,6-naphthyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; iron / water; ethanol / 2 h / 50 °C / Reflux

2: trifluoroacetic acid; caesium carbonate

With hydrogenchloride; iron; caesium carbonate; trifluoroacetic acid; In ethanol; water;