Technology Process of C52H79NO16
There total 7 articles about C52H79NO16 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
osmium(VIII) oxide; 4-methylmorpholine N-oxide;
In
water; acetone; tert-butyl alcohol;
at 20 ℃;
for 4h;
DOI:10.1021/jm051157a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 90 percent / pyridinium p-toluenesulfonate / acetonitrile; H2O / 17 h / 68 °C
2: 82 percent / N-methylmorpholine N-oxide monohydrate; OsO4 / acetone; 2-methyl-propan-2-ol; H2O / 4 h / 20 °C
With
osmium(VIII) oxide; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide;
In
water; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm051157a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 g / pyridinium p-toluenesulfonate / acetone / 18 h / 60 °C
2: 44 g / thionyl chloride; Et3N / ethyl acetate / 2 h / 0 °C
3: 90 percent / pyridinium p-toluenesulfonate / acetonitrile; H2O / 17 h / 68 °C
4: 82 percent / N-methylmorpholine N-oxide monohydrate; OsO4 / acetone; 2-methyl-propan-2-ol; H2O / 4 h / 20 °C
With
osmium(VIII) oxide; thionyl chloride; pyridinium p-toluenesulfonate; 4-methylmorpholine N-oxide; triethylamine;
In
water; ethyl acetate; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm051157a