4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone

Base Information

Chemical Name:4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone
CAS No.:142874-91-7
Molecular Formula:C₁₉H₂₀ClNO
Molecular Weight:313.827
Hs Code.:

Synonyms:4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone

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Chemical Property of 4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone

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Technology Process of 4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone

There total 1 articles about 4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 60404-95-7
3,5,6-trimethyl-2-(2-methyl-2-propenyl)-1,4-benzoquinone

: 106-47-8
4-chloro-aniline

: 142874-91-7
4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone

Guidance literature:: With pyridine; titanium tetrachloride; In 1,2-dichloro-ethane; at 90 ℃; for 0.75h;
DOI:10.1021/jm960411j

Reference yield:

: 142874-91-7
4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone

: 142874-93-9
4-(4-Chlorophenylamino)-3,5,6-trimethyl-2-(2-methyl-2-propenyl)phenol

Guidance literature:: With sodium dithionite; In tetrahydrofuran; for 0.5h; Ambient temperature;
DOI:10.1021/jm960411j

Reference yield:

: 142874-91-7
4-[(E)-4-Chloro-phenylimino]-2,3,5-trimethyl-6-(2-methyl-allyl)-cyclohexa-2,5-dienone

: 5-(4-Chlorophenylamino)-2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: aq. Na₂S₂O₄ / tetrahydrofuran / 0.5 h / Ambient temperature

2: 60 percent / 35percent aq. HCl / methanol / 2 h / Heating

With hydrogenchloride; sodium dithionite; In tetrahydrofuran; methanol;
DOI:10.1021/jm960411j