(η5-C5Me4-3,5-Me2C6H3)2TiCl

Base Information

Chemical Name:(η5-C5Me4-3,5-Me2C6H3)2TiCl
CAS No.:1173710-75-2
Molecular Formula:C₃₄H₄₂ClTi
Molecular Weight:534.04
Hs Code.:

Synonyms:(η5-C5Me4-3,5-Me2C6H3)2TiCl

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Chemical Property of (η5-C5Me4-3,5-Me2C6H3)2TiCl

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Technology Process of (η5-C5Me4-3,5-Me2C6H3)2TiCl

There total 1 articles about (η5-C5Me4-3,5-Me2C6H3)2TiCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 31168-87-3,18039-90-2
titanium trichloride tris(tetrahydrofuran)

: Li⁽¹⁺⁾*C₅(CH₃)4C₆H₃(CH₃)2^(1-)=Li(C₅(CH₃)4C₆H₃(CH₃)2)

: 1173710-75-2
(η5-C5Me4-3,5-Me2C6H3)2TiCl

Guidance literature:: In tetrahydrofuran; THF added by vac. transfer at -78°C to mixt. of Li compd. and Ti complex; warmed to ambient temp. with stirring; refluxed for 60 h; solvent removed in vac.; dissolved in pentane; filtered through Celite; solvent removed in vac.; recrystd. from pentane; elem. anal.;
DOI:10.1021/om900282u

Reference yield: 90.0%

: 1173710-75-2
(η5-C5Me4-3,5-Me2C6H3)2TiCl

: 1173710-54-7
(η5-C5Me4-3,5-Me2C6H3)2Ti

Guidance literature:: With sodium amalgam; In toluene; byproducts: NaCl; toluene soln. of Ti complex added to sodium amalgam and toluene with stirring; stirred at ambient temp. for 3 d; filtered through Celite; solvent removed in vac.; recrystd. from pentane; elem. anal.;
DOI:10.1021/om900282u