5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenzanthracene

Base Information

• Chemical Name: 5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenz
• Molecular Formula: C₃₉H₃₈O₆
• Molecular Weight: 602.727

Synonyms:5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenzanthracene

Chemical Property of 5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenz

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

There total 1 articles about 5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenzanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

O-benzoyl-α-(1-phenyl-3-methyl-6,7-dimethoxyisochromen-1-yl)-3,4-dimethoxyphenylacetone (135330-81-3) → 5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenzanthracene (121275-98-7)

Guidance literature:

With sodium hydroxide; In isopropyl alcohol; for 0.25h; Heating;

DOI:10.1007/BF00474039

Reference yield: 97.0%

5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenzanthracene (121275-98-7) → 5,12-diphenyl-7-acetyl-2,3,9,10-tetramethoxybenzanthracene (121275-99-8)

Guidance literature:

In acetic acid; Heating;

DOI:10.1007/BF00474039

Reference yield:

5,12-diphenyl-7-acetyl-12-isopropoxy-2,3,9,10-tetramethoxy-12,12a-dihydrobenzanthracene (121275-98-7) → 5,12-diphenyl-2,3,9,10-tetramethoxybenzanthracene (121262-26-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / acetic acid / Heating

2: 80 percent / trifluoroacetic acid / 48 h

In acetic acid; trifluoroacetic acid;

DOI:10.1007/BF00474039

upstream raw materials:

O-benzoyl-α-(1-phenyl-3-methyl-6,7-dimethoxyisochromen-1-yl)-3,4-dimethoxyphenylacetone

Downstream raw materials:

5,12-diphenyl-7-acetyl-2,3,9,10-tetramethoxybenzanthracene

5,12-diphenyl-2,3,9,10-tetramethoxybenzanthracene

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