μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol

Base Information

• Chemical Name: μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol
• CAS No.: 90443-69-9
• Molecular Formula: C₂₄H₂₀B*C₅₁H₄₆ClN₂O₃P₄Rh₂
• Molecular Weight: 1419.33

Synonyms:μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol

Chemical Property of μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol

Chemical Property:

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Technology Process of μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol

There total 1 articles about μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

μ-carbonyl-μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol → μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol (90443-69-9)

Guidance literature:

With CH₃OH; In methanol; byproducts: CO; complex soln. stirred at room temp. under vac.; filtered, washed (Et2O), dried (vac.); elem. anal.;

DOI:10.1016/0022-328X(84)85034-2

Reference yield: 94.0%

diethyl ether (60-29-7,927820-24-4) + μ-chloro-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate-methanol (90443-69-9) → μ-chloro-μ-dichloromethane-di[μ-bis(diphenylphosphino)amine-P,P']-bis[carbonyl-rhodium(I)]-tetraphenylborate diethyl ether

Guidance literature:

With CH₂Cl₂; In dichloromethane; (N2); complex in CH2Cl2 dissolved, at room temp. for 2 h stirred under vac.; crystd. (Et2O at -18°C), filtered, washed with Et2O, dried (vac.); elem. anal.;

DOI:10.1016/0022-328X(84)85034-2

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