2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

Base Information

Chemical Name:2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside
CAS No.:1033706-60-3
Molecular Formula:C₆₈H₆₈O₁₈Si
Molecular Weight:1201.36
Hs Code.:

Synonyms:2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

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Chemical Property of 2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

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Technology Process of 2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

There total 1 articles about 2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1033706-58-9
2'-(benzyloxycarbonyl)benzyl (2,3,5-tri-O-benzoyl-6-O-t-buthyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

: 1033706-60-3
2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

Guidance literature:: With palladium dihydroxide; ammonium acetate; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol800530u

Reference yield: 88.0%

: 1033706-60-3
2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside

: 1033706-61-4
(2,3,5-tri-O-benzoyl-6-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranosyl fluoride

Guidance literature:: 2'-carboxybenzyl (2,3,5-tri-O-benzoyl-6-O-t-butyldimethylsilyl-β-D-galactofuranosyl)-(1->5)-2,3-di-O-benzoyl-6-O-benzyl-β-D-galactofuranoside; With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

With pyridine; trifluoromethylsulfonic anhydride; hydrogen fluoride; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at -78 - 0 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol800530u