4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside

Base Information

Chemical Name:4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside
CAS No.:845271-56-9
Molecular Formula:C₁₉H₂₀F₃NO₁₃S
Molecular Weight:559.428
Hs Code.:

Synonyms:4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside

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Chemical Property of 4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside

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Technology Process of 4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside

There total 3 articles about 4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 87236-45-1
4-nitrophenyl 3,4,6-tri-O-acetyl-β-D-glucopyranoside

: 845271-56-9
4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside

Guidance literature:: In pyridine; dichloromethane; at 3 - 20 ℃;
DOI:10.1016/j.carres.2004.11.002

Reference yield:

: 53872-80-3
bromure de tri-O-acetyl-3,4,6-α-D-glucopyranosyle

: 845271-56-9
4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 3.84 g / K₂CO₃ / acetone / 16 h / 20 °C

2: 84 percent / CH₂Cl₂; pyridine / 3 - 20 °C

With potassium carbonate; In pyridine; dichloromethane; acetone;
DOI:10.1016/j.carres.2004.11.002

Reference yield:

: 4692-12-0
1,3,4,6-tetra-O-acetyl glucopyranose

: 845271-56-9
4-nitrophenyl 3,4,6-tri-O-acetyl-2-O-trifluoromethanesulfonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / HBr / CH₂Cl₂ / 3 h / 3 °C

2: 3.84 g / K₂CO₃ / acetone / 16 h / 20 °C

3: 84 percent / CH₂Cl₂; pyridine / 3 - 20 °C

With hydrogen bromide; potassium carbonate; In pyridine; dichloromethane; acetone;
DOI:10.1016/j.carres.2004.11.002