5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole

Base Information

Chemical Name:5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole
CAS No.:1379669-27-8
Molecular Formula:C₂₂H₂₆O₈
Molecular Weight:418.444
Hs Code.:

Synonyms:5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole

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Chemical Property of 5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole

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Technology Process of 5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole

There total 3 articles about 5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1379669-23-4
(6-[1,3]dioxan-2-ylbenzo[1,3]dioxolan-5-yl)-(3,4,5-trimethoxyphenyl)methanol

: 1379669-27-8
5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole

Guidance literature:: (6-[1,3]dioxan-2-ylbenzo[1,3]dioxolan-5-yl)-(3,4,5-trimethoxyphenyl)methanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h;

halomethane; In tetrahydrofuran; mineral oil; at 20 ℃; for 18h;
DOI:10.1002/chem.201101909

Reference yield:

: 86449-40-3
1-<1-(2-bromo-4,5-methylenedioxyphenyl)>-1,3-dioxane

: 1379669-27-8
5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

2.2: 18 h / 20 °C

With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; mineral oil;
DOI:10.1002/chem.201101909

Reference yield:

: 15930-53-7
6-bromo-3,4-methylenedioxybenzaldehyde

: 1379669-27-8
5-[methoxy-(3,4,5-trimethoxyphenyl)methyl]-6-[1,3]dioxane-2-ylbenzo[1,3]dioxole

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / benzene / 4 h / Reflux

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

3.2: 18 h / 20 °C

With n-butyllithium; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; mineral oil; benzene;
DOI:10.1002/chem.201101909