(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

Base Information

Chemical Name:(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone
CAS No.:1407164-57-1
Molecular Formula:C₂₈H₃₁N₃O₆Si
Molecular Weight:533.656
Hs Code.:

Synonyms:(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

Chemical Property:

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Technology Process of (2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

There total 2 articles about (2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132047-92-8
tert-butyl(pent-4-en-1-yloxy)diphenylsilane

: 1407164-57-1
(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: chloramine T trihydrate; phenyltrimethylammonium tribromide / acetonitrile / 12 h / Inert atmosphere

2: sodium naphthalenide / 1,2-dimethoxyethane / -78 °C / Inert atmosphere

3: acetonitrile / 1.5 h / 0 - 20 °C / Inert atmosphere

With phenyltrimethylammonium tribromide; chloramine T trihydrate; sodium naphthalenide; In 1,2-dimethoxyethane; acetonitrile;
DOI:10.1002/anie.201204224

Reference yield:

: C₂₁H₂₉NOSi

: 87581-19-9
2,5-dioxopyrrolidin-1-yl 3,5-dinitrobenzoate

: 1407164-57-1
(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

Guidance literature:: In acetonitrile; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/anie.201204224

Reference yield: 49.0%

: 1407164-57-1
(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

: (S)-(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

: 1407164-58-2
(R)-(2-(3-((tert-butyldiphenylsilyl)oxy)propyl)aziridin-1-yl)(3,5-dinitrophenyl)methanone

Guidance literature:: With triphenylborane; (R)-1,1'-Bi-2-naphthol; In dichloromethane; at -30 ℃; for 3h; Inert atmosphere;
DOI:10.1002/anie.201204224