N-cyclohexyl-i-propyl-butylhydrazone

Base Information

Chemical Name:N-cyclohexyl-i-propyl-butylhydrazone
CAS No.:935753-46-1
Molecular Formula:C₁₃H₂₆N₂
Molecular Weight:210.363
Hs Code.:

Synonyms:N-cyclohexyl-i-propyl-butylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-cyclohexyl-i-propyl-butylhydrazone

Chemical Property:

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Technology Process of N-cyclohexyl-i-propyl-butylhydrazone

There total 3 articles about N-cyclohexyl-i-propyl-butylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 32400-20-7
lithium cyclohexylisopropylamide

: 935753-46-1
N-cyclohexyl-i-propyl-butylhydrazone

: 1195-42-2
N-cyclohexylisopropylamine

: 71302-63-1
N-nitroso-isopropylcyclohexylamine

Guidance literature:: lithium cyclohexylisopropylamide; With nitrogen(II) oxide; In tetrahydrofuran; at -19 - 0 ℃; for 3h; under 759.826 Torr;

n-butyllithium; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/poc.1451

Reference yield:

: 1195-42-2
N-cyclohexylisopropylamine

: 935753-46-1
N-cyclohexyl-i-propyl-butylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / hexane

1.2: 80 percent / nitric oxide / tetrahydrofuran / 3 h / 759811 Torr / cooling

2.1: hexane

With n-butyllithium; In hexane;
DOI:10.1002/poc.1069