(E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester

Base Information

Chemical Name:(E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester
CAS No.:146233-13-8
Molecular Formula:C₂₅H₂₆N₂O₇
Molecular Weight:466.491
Hs Code.:

Synonyms:(E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester

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Chemical Property of (E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester

Chemical Property:

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Technology Process of (E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester

There total 3 articles about (E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 146233-07-0
ethyl 3-benzoylamino-6-(3,4-dimethoxy-6-nitrostyryl)-2-oxo-2H-pyran-5-carboxylate

: N-(8,9-Dimethoxy-2,5-dioxo-5,6,11,12-tetrahydro-2H-1-oxa-6-aza-dibenzo[a,e]cycloocten-3-yl)-benzamide

: 146233-13-8
(E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 735.5 Torr; Ambient temperature;

Reference yield:

: 20357-25-9
6-nitroveratraldehyde

: 146233-13-8
(E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / toluene / Heating

2: 53 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 735.5 Torr / Ambient temperature

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; toluene;

Reference yield:

: 142503-18-2
ethyl-3-(benzoylamino)-2-oxo-6-(triphenylphosphoranylidenemethyl)-2H-pyran-5-carboxylate

: 146233-13-8
(E)-2-Benzoylamino-4-[6,7-dimethoxy-3,4-dihydro-1H-quinolin-(2E)-ylidene]-pent-2-enedioic acid 5-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / toluene / Heating

2: 53 percent / H₂ / 10percent Pd/C / tetrahydrofuran / 735.5 Torr / Ambient temperature

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; toluene;