Technology Process of C38H36N2O3S
There total 4 articles about C38H36N2O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
chloro(1,5-cyclooctadiene)rhodium(I) dimer; sodium ethanolate;
In
ethanol; dichloromethane;
at 0 ℃;
for 18h;
optical yield given as %de;
Inert atmosphere;
Molecular sieve;
DOI:10.1021/ol201438k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: titanium(IV) isopropylate / dichloromethane / 20 °C / Inert atmosphere
2: chloro(1,5-cyclooctadiene)rhodium(I) dimer; sodium ethanolate / ethanol; dichloromethane / 18 h / 0 °C / Inert atmosphere; Molecular sieve
With
titanium(IV) isopropylate; chloro(1,5-cyclooctadiene)rhodium(I) dimer; sodium ethanolate;
In
ethanol; dichloromethane;
DOI:10.1021/ol201438k
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.58 h / 0 - 20 °C / Inert atmosphere
1.2: 6 h / Inert atmosphere
2.1: titanium(IV) isopropylate / dichloromethane / 20 °C / Inert atmosphere
3.1: chloro(1,5-cyclooctadiene)rhodium(I) dimer; sodium ethanolate / ethanol; dichloromethane / 18 h / 0 °C / Inert atmosphere; Molecular sieve
With
titanium(IV) isopropylate; chloro(1,5-cyclooctadiene)rhodium(I) dimer; sodium ethanolate; sodium hydride;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol201438k