1-(2-fluorophenyl)allyl but-3-enoate

Base Information

Chemical Name:1-(2-fluorophenyl)allyl but-3-enoate
CAS No.:1374313-50-4
Molecular Formula:C₁₃H₁₃FO₂
Molecular Weight:220.243
Hs Code.:

Synonyms:1-(2-fluorophenyl)allyl but-3-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-fluorophenyl)allyl but-3-enoate

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Technology Process of 1-(2-fluorophenyl)allyl but-3-enoate

There total 1 articles about 1-(2-fluorophenyl)allyl but-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 625-38-7
but-3-enoic acid

: 58824-51-4
1-(2-fluorophenyl)-2-propen-1-ol

: 1374313-50-4
1-(2-fluorophenyl)allyl but-3-enoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201101497

Reference yield: 86.0%

: 1374313-50-4
1-(2-fluorophenyl)allyl but-3-enoate

: 1376703-43-3
6-(2-fluorophenyl)-5,6-dihydropyran-2-one

Guidance literature:: 1-(2-fluorophenyl)allyl but-3-enoate; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 65 - 80 ℃; Inert atmosphere;

With triethylsilane; In toluene; at 110 ℃; Inert atmosphere;
DOI:10.1055/s-0031-1290488

Reference yield: 75.0%

: 1374313-50-4
1-(2-fluorophenyl)allyl but-3-enoate

: 368-39-8
triethyloxonium fluoroborate

: (2Z,4E)-ethyl 5-(2-fluorophenyl)penta-2,4-dienoate

Guidance literature:: 1-(2-fluorophenyl)allyl but-3-enoate; With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 80 ℃; Inert atmosphere; Schlenk technique;

With sodium hydride; In toluene; mineral oil; at 80 ℃; Inert atmosphere; Schlenk technique;

triethyloxonium fluoroborate; In toluene; mineral oil; at 0 - 20 ℃; Solvent; stereoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1055/s-0035-1562536